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Center for Optical Materials Science and Engineering Technologies (COMSET)

Facilities

Clemson has made a major commitment to support the Center for Optical Materials Science and Engineering Technologies (COMSET), whose mission is to become a global leader for innovation and education in the science and technology of optical materials and optoelectronics, through research, teaching and the transfer and expansion of optical technologies to the private and public sector. COMSET is headquartered at the Advanced Materials Research Laboratory (AMRL), a $21 million state-of-the-art laboratory located at the Advanced Materials Center in Anderson, S.C.

The building

In specific regards to optical fiber fabrication, COMSET operates an Optical Fiber Laboratory, which is the only academic facility in the United States with industry-grade capabilities for fabricating optical fiber. As is detailed below, the Optical Fiber Laboratory comprises an SG Controls MCVD lathe and Heathway Fiber Draw Tower along with a preform and fiber characterization laboratory. The draw tower, lathe and a staff of three on-site researchers with more than 40 years of cumulative industrial experience in the optical fiber industry uniquely position Clemson for defense-related basic research into optical fibers.

Lathe Modified Chemical Vapor Deposition (MCVD) Lathe

The SG Controls MCVD lathe has an extended bed with a motorized tailstock and double jaw chucks on both headstock and tailstock capable of securing glass preform stock up to 1.5 meters in length and 70 mm in diameter. The temperature of the preform is monitored with a tracking pyrometer that provides feedback for flow to a half-round hydrogen/oxygen torch with a nitrogen curtain capability, all of which is housed in a clean room enclosure with air flow control.

The lathe is interfaced through QNX software using a recipe-based control for all process variables. This allows for carriage speed, mass flow and tube temperature changes to be set or modified at any time during the process. Liquid precursors are delivered to one of four bubblers with individual oil bath control and isothermal heaters to maintain constant temperature. Additional gases are routed through a gas drier/purifier system using electro-polished stainless steel tubing. The lathe is plumbed for N2, O2, H2, Cl2, He, SF6, SiF4, Freon, BCl3, SiCl4, GeCl4, POCl3, two additional spare gases and one spare liquid precursor.

Tower Optical Fiber Draw Tower

The Heathway 6.5 meter optical fiber draw tower is equipped with three interchangeable furnaces that can cover a range of temperatures from ambient to 2200 ºC. These furnaces include a high temperature graphite resistance furnace capable of a maximum temperature of 2200 ºC, which is most often used to draw silica materials. This high temperature furnace also has an interchangeable graphite element package to accommodate preforms up to 50 mm in diameter. An inert argon atmosphere inside the furnace protects the graphite form oxidizing during high temperature use. The two intermediate temperature furnaces are used for soft glasses and polymer draws.

The Clemson draw tower is capable of handling preforms from less than 5 to 50 mm. Line speeds up to 180 m/min are possible with forced cooling needed above ~ 80 m/min. Laminar HEPA filtered air flows across the draw line to maintain a particulate free environment. Dual diameter gauges, before and after coating, accurately monitor fiber diameters from 30 to greater than 6000 mm. The tower is also equipped with an automatic preform x-y adjustment unit. Two tractor units provide additional pulling capacity on the tower. A starter tractor assembly draws the fiber at a steady rate and at a consistent diameter for feeding the fiber into the solid die coating systems. A cane tractor assembly provides the capability of drawing rod or tubes of diameters from 500 to 6000 microns.

Central  Instrumental Resources

Jobin Horbia Jobin Yvon Horiba – Fluorolog 3-222 – Tau 3 / TCSPC photoluminescence spectrophotometer

  • Excitation range
    • 200nm – 1200nm, via xenon bulb and monochromator
  • UV-Vis detector range
    • 200nm – 800nm, via Horiba visible 400381 pmt
  • NIR detector range
    • 900nm – 1700nm, via Hamamatsu H10330A-75 pmt
  • Lifetime range
    • 10ps – 10µm, via Tau lifetime
      • Using a Amplifier Research 25A250AM6 amplifier
    • 6ns – 1µm, via Time Correlated Single Photon Counter (TCSPC) with nanoLED
    • 50µm – tens of seconds, via Phosphorescence with xenon flash lamp
  • Sample range
    • Solutions, Bulk, Films, Aggregates, and Powders
    • Sample can be front facing or at a right angle to the light source
    • 3 sample holders
      • Standard for liquid or solid
      • Low temperature holder with a liquid N2 dewar
      • Thermostating holder that can switch between two samples in quartz cuvettes
  • Software
    • FluorEssence
    • DataMax
    • Data Station for TCSPC
    • DAS6 for TCSPC

Lambda Perkin Elmer – Lambda 900 – UV/Vis/NIR Spectrometer

  • Scanning range
    • 185nm – 3300nm
      • ±0.08nm UV/Vis, via deuterium and halogen lamps with a photomultiplier detector
      •  ±0.32nm NIR, via halogen lamp with a Peltier-cooled PbS detector
  • Sample Range
    • Solutions, and solids
  • Software
    • UV WinLab

Photon Technology International Inc. (PTI) Photon Technology International Inc. (PTI) Fluorescence Master Systems – Quanta Master 60 – Flourometer

  • Excitation Range
    • 180nm – 1200nm, via xenon lamp
  • Emission Detection Range
    • 200nm – 1800nm, via Hamamatsu pmt with C9940 cooler
  • Sample Range
    • Solution and solids
      • Has a motorized sample stirrer
      • Has a thermostable cuvette holder
  • Software
    • FelixGX

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